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An analytical method for the determination of perfluorinated compounds in whole blood using acetonitrile and solid phase extraction methods
National Institute of Advanced Industrial Science and Technology (AIST), 16-1 Onogawa, Tsukuba, Ibaraki, Japan; Department of Biology and Chemistry, City University of Hong Kong, Tat Chee Avenue, Kowloon, Hong Kong SAR, People’s Republic of China.ORCID iD: 0000-0001-6800-5658
National Institute of Advanced Industrial Science and Technology (AIST), 16-1 Onogawa, Tsukuba, Ibaraki, Japan.
cWadsworth Center, New York State Department of Health and Department of Environmental Health Sciences, State University of New York at Albany, Empire State Plaza, Albany, NY, USA.
Department of Biology and Chemistry, City University of Hong Kong, Tat Chee Avenue, Kowloon, Hong Kong SAR, People’s Republic of China.
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2009 (English)In: Journal of Chromatography A, ISSN 0021-9673, E-ISSN 1873-3778, Vol. 1216, no 25, p. 4950-4956Article in journal (Refereed) Published
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Abstract [en]

A method for the analysis of perfluorinated compounds (perfluoroalkyl sulfonates: C4, C6, C8, C10; perfluoroalkyl sulfinates: C6, C8, C10; perfluorooctanesulfonamide, N-ethyl perfluorooctanesulfonamide, N-ethyl perfluorooctanesulfonamidoacetate, perfluorocarboxylates: C4–C14; fluorotelomer carboxylate (7:3, 8:2) in whole blood using acetonitrile and OASIS WAX® solid phase extraction (SPE) cartridge was developed. Separation of target compounds in two HPLC columns (ion exchange JJ50-2D and C18 Betasil columns) was examined. Matrix recoveries of the developed methods ranged from 70% to 120%. Separation of possible inferences such as taurodeoxycholic acid (TDC) was accomplished using an ion exchange JJ50-2D column, and this separation was validated using whole blood of different animals.

Place, publisher, year, edition, pages
Amsterdam, Netherlands: Elsevier, 2009. Vol. 1216, no 25, p. 4950-4956
Keywords [en]
Whole blood, Acetonitrile, Solid phase extraction, Formic acid, Taurodeoxycholic acid, Perfluorooctanesulfonate
National Category
Environmental Sciences
Identifiers
URN: urn:nbn:se:oru:diva-49989DOI: 10.1016/j.chroma.2009.04.070ISI: 000267086400003PubMedID: 19439311Scopus ID: 2-s2.0-65649149109OAI: oai:DiVA.org:oru-49989DiVA, id: diva2:950415
Note

Funding Agency:

City University of Hong Kong 

Available from: 2016-07-29 Created: 2016-04-28 Last updated: 2017-11-28Bibliographically approved

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Yeung, Leo W. Y.Lam, Paul K. S.

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